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MAT253-Kiel Device Data Log



On-Line Psuedo-Realtime 253-Kiel Data

Date Time Row Line Pos. Sample ID Wt. (µg) S. Int (mV) Int. S/R δ13C ± 1σ δ18O ± 1σ
06/18/1100:06:514622446. NBS1902,3770.982.020.05-2.240.05
06/18/1100:06:514622446. NBS1902,3770.982.020.05-2.240.05
0.000.000.000.00
0.000.000.000.00
0.000.000.000.00
0.000.000.000.00
0.000.000.000.00
0.000.000.000.00




MAT253-Kiel Device Run Log File



[0 ][(06/21/11 16:55:26) 같같같같같같같같같같][같같]
[13 ][(07/13/11 10:11:31) Turret position ( 1) Ok!][]
[6 ][(07/13/11 10:11:36) Disconnected vial at Line 1 / Position 1 ][]
[13 ][(07/13/11 10:11:41) Turret position ( 1) Ok!][]
[6 ][(07/13/11 10:11:45) Disconnected vial at Line 2 / Position 1 ][]
[13 ][(07/13/11 10:12:11) Turret position ( 2) Ok!][]
[6 ][(07/13/11 10:12:19) Connected vial at Line 1 /Position 2 ][]
[2 ][(07/13/11 10:12:24) No Response from Microswitch (Missing Vial ?) Line: 2][]
[0 ][(07/13/11 10:12:24) Can not open Valve 23: No Vial connected][]
[0 ][(07/13/11 10:12:27) Vial not connected on Line 2 Sample 2 ][]
[17 ][(07/13/11 10:12:27) START DROPPING TEST][]
[0 ][(07/13/11 10:12:44) started Standby][]
[0 ][(07/13/11 10:12:44) executed Standby][]
[1 ][(07/13/11 10:12:44) ][]
[1 ][(07/13/11 10:12:44) An NORMAL Error occured : ][]
[13 ][(07/13/11 10:13:08) Turret position ( 2) Ok!][]
[6 ][(07/13/11 10:13:13) Disconnected vial at Line 1 / Position 2 ][]
[13 ][(07/13/11 10:13:38) Turret position ( 1) Ok!][]
[2 ][(07/13/11 10:14:19) No Response from Microswitch (Missing Vial ?) Line: 2][]
[0 ][(07/13/11 10:14:19) Can not open Valve 23: No Vial connected][]
[0 ][(07/13/11 10:14:21) Vial not connected on Line 2 Sample 1 ][]
[2 ][(07/13/11 10:15:12) No Response from Microswitch (Missing Vial ?) Line: 2][]
[0 ][(07/13/11 10:15:12) Can not open Valve 23: No Vial connected][]
[0 ][(07/13/11 10:15:15) Vial not connected on Line 2 Sample 1 ][]
[2 ][(07/13/11 10:15:46) No Response from Microswitch (Missing Vial ?) Line: 2][]
[0 ][(07/13/11 10:15:47) Can not open Valve 23: No Vial connected][]
[0 ][(07/13/11 10:15:49) Vial not connected on Line 2 Sample 1 ][]
[2 ][(07/13/11 10:15:59) No Response from Microswitch (Missing Vial ?) Line: 2][]
[0 ][(07/13/11 10:16:00) Can not open Valve 23: No Vial connected][]
[0 ][(07/13/11 10:16:02) Vial not connected on Line 2 Sample 1 ][]
[2 ][(07/13/11 10:16:12) No Response from Microswitch (Missing Vial ?) Line: 2][]
[0 ][(07/13/11 10:16:12) Can not open Valve 23: No Vial connected][]
[0 ][(07/13/11 10:16:14) Vial not connected on Line 2 Sample 1 ][]
[2 ][(07/13/11 10:16:26) No Response from Microswitch (Missing Vial ?) Line: 2][]
[0 ][(07/13/11 10:16:26) Can not open Valve 23: No Vial connected][]
[0 ][(07/13/11 10:16:29) Vial not connected on Line 2 Sample 1 ][]
[13 ][(07/13/11 10:17:04) Turret position ( 2) Ok!][]
[6 ][(07/13/11 10:17:11) Connected vial at Line 1 /Position 2 ][]
[6 ][(07/13/11 10:17:18) Connected vial at Line 2 /Position 2 ][]
[17 ][(07/13/11 10:17:18) START DROPPING TEST][]
[2 ][(07/13/11 10:19:18) One Drop: No Acid Detected during timeout period][]
[0 ][(07/13/11 10:19:18) Dropping Error Line: 1 Drop: 1][]
[0 ][(07/13/11 10:19:18) started Standby][]
[0 ][(07/13/11 10:19:18) executed Standby][]
[1 ][(07/13/11 10:19:18) ][]
[1 ][(07/13/11 10:19:18) An NORMAL Error occured : ][]
[13 ][(07/13/11 10:19:43) Turret position ( 2) Ok!][]
[6 ][(07/13/11 10:19:49) Disconnected vial at Line 1 / Position 2 ][]
[13 ][(07/13/11 10:19:53) Turret position ( 2) Ok!][]
[6 ][(07/13/11 10:19:59) Disconnected vial at Line 2 / Position 2 ][]
[13 ][(07/13/11 10:20:16) Turret position ( 1) Ok!][]
[13 ][(07/13/11 10:45:31) Turret position ( 2) Ok!][]
[6 ][(07/13/11 10:45:38) Connected vial at Line 1 /Position 2 ][]
[6 ][(07/13/11 10:45:46) Connected vial at Line 2 /Position 2 ][]
[17 ][(07/13/11 10:45:46) START DROPPING TEST][]
[0 ][(07/13/11 10:45:46) Drop detected Line: 1 Drop: 1][]
[0 ][(07/13/11 10:46:15) Drop detected Line: 2 Drop: 1][]
[0 ][(07/13/11 10:46:15) Drop detected Line: 1 Drop: 2][]
[0 ][(07/13/11 10:46:33) Drop detected Line: 2 Drop: 2][]
[0 ][(07/13/11 10:46:36) Drop detected Line: 1 Drop: 3][]
[0 ][(07/13/11 10:46:36) Drop detected Line: 2 Drop: 3][]
[0 ][(07/13/11 10:46:37) Drop detected Line: 1 Drop: 4][]
[0 ][(07/13/11 10:46:38) Drop detected Line: 2 Drop: 4][]
[0 ][(07/13/11 10:46:38) Drop detected Line: 1 Drop: 5][]
[0 ][(07/13/11 10:46:38) Drop detected Line: 2 Drop: 5][]
[13 ][(07/13/11 10:46:38) Turret position ( 2) Ok!][]
[6 ][(07/13/11 10:46:43) Disconnected vial at Line 1 / Position 2 ][]
[13 ][(07/13/11 10:46:49) Turret position ( 2) Ok!][]
[6 ][(07/13/11 10:46:54) Disconnected vial at Line 2 / Position 2 ][]
[13 ][(07/13/11 10:47:12) Turret position ( 1) Ok!][]
[6 ][(07/13/11 10:47:20) Connected vial at Line 1 /Position 1 ][]
[6 ][(07/13/11 10:47:27) Connected vial at Line 2 /Position 1 ][]
[0 ][(07/13/11 10:47:27) started Standby][]
[0 ][(07/13/11 10:47:27) executed Standby][]
[13 ][(07/13/11 10:47:41) Turret position ( 1) Ok!][]
[6 ][(07/13/11 10:47:47) Disconnected vial at Line 1 / Position 1 ][]
[13 ][(07/13/11 10:47:51) Turret position ( 1) Ok!][]
[6 ][(07/13/11 10:47:57) Disconnected vial at Line 2 / Position 1 ][]
[13 ][(07/13/11 10:48:02) Turret position ( 1) Ok!][]
[13 ][(07/13/11 10:56:51) Turret position ( 1) Ok!][]
[6 ][(07/13/11 10:56:59) Connected vial at Line 1 /Position 1 ][]
[6 ][(07/13/11 10:57:06) Connected vial at Line 2 /Position 1 ][]
[6 ][(07/13/11 11:30:54) 0 files saved.][]
[31 ][(07/13/11 11:30:54) Result Path][C:\Thermo\Isodat NT\Global\User\Dual Inlet System\Results\ACQ-Results\Kate_Littler\]
[16 ][(07/13/11 11:30:55) Sample ISL Script 0][]
[1 ][(07/13/11 11:30:56) CleanUp Script terminates now][]
[17 ][(07/13/11 11:30:56) Start New Carbonate Acquisition script][]
[17 ][(07/13/11 11:30:57) PR: Prepare Run - Start][]
[17 ][(07/13/11 11:30:57) PR: Set COV valves OFF:22,13,15,26,39; ON:16,40.][]
[0 ][(07/13/11 11:30:57) PR: Pump COV Sample Side 10 (Sec) ][]
[17 ][(07/13/11 11:31:07) PR: Set COV to standard; OFF:13,16,40; ON:25.][]
[17 ][(07/13/11 11:31:09) PR: Initialize turret.][]
[13 ][(07/13/11 11:31:09) Turret position ( 1) Ok!][]
[6 ][(07/13/11 11:31:15) Disconnected vial at Line 1 / Position 1 ][]
[13 ][(07/13/11 11:31:19) Turret position ( 1) Ok!][]
[6 ][(07/13/11 11:31:25) Disconnected vial at Line 2 / Position 1 ][]
[13 ][(07/13/11 11:31:30) Turret position ( 1) Ok!][]
[6 ][(07/13/11 11:31:37) Connected vial at Line 1 /Position 1 ][]
[6 ][(07/13/11 11:31:44) Connected vial at Line 2 /Position 1 ][]
[17 ][(07/13/11 11:31:44) PR: Initialize Kiel valves, ON:2,3,4,5; OFF:1.][]
[17 ][(07/13/11 11:31:44) PR: Bakeout T1 and T2][]
[0 ][(07/13/11 11:31:44) Set Trap 1 to 140 (캜)][]
[0 ][(07/13/11 11:31:44) Set Trap 2 to 140 (캜)][]
[0 ][(07/13/11 11:33:46) Set Trap 1 to 140 (캜)][]
[17 ][(07/13/11 11:38:46) PR: Filling LN2 Reservoir...][]
[18 ][(07/13/11 11:40:04) PR: Prepare Run finished][]
[16 ][(07/13/11 11:40:04) Start PREPARATION Script 0][]
[17 ][(07/13/11 11:40:04) P: Start Preparing Line 1 Position 2][]
[0 ][(07/13/11 11:40:04) Set Trap 2 to 30 (캜)][]
[0 ][(07/13/11 11:40:04) P: Wait for Trap 1 free][]
[17 ][(07/13/11 11:40:04) M: Start Measuring Line 1 Sample 2 - Wait for Prep ready][]
[0 ][(07/13/11 11:40:06) Set Trap 1 to 140 (캜)][]
[17 ][(07/13/11 11:40:12) P: Start pumping Trap 1 for 75 s with Kiel valves 1 and 2 OFF.][]
[17 ][(07/13/11 11:41:27) P: Continue pumping Trap 1 for 75 s with Kiel valves 1 and 2 ON.][]
[0 ][(07/13/11 11:42:42) Acid Temperature: 77.4 (캜)][]
[0 ][(07/13/11 11:42:42) P: Connecting sample vial (line 1, position 2)...][]
[13 ][(07/13/11 11:42:43) Turret position ( 1) Ok!][]
[6 ][(07/13/11 11:42:48) Disconnected vial at Line 1 / Position 1 ][]
[13 ][(07/13/11 11:42:53) Turret position ( 2) Ok!][]
[6 ][(07/13/11 11:43:01) Connected vial at Line 1 /Position 2 ][]
[17 ][(07/13/11 11:43:01) LT: Starting leak test.][]
[17 ][(07/13/11 11:43:01) LT: Pumpdown sample for 150 s...][]
[1 ][(07/13/11 11:45:31) LT: Wait to reach 1000.0 (킶ar)][]
[18 ][(07/13/11 11:46:13) LT: Leak test finished. LeakRate : 278.4 킖ar/Min][]
[0 ][(07/13/11 11:46:13) Set Trap 1 to -20 (캜)][]
[0 ][(07/13/11 11:47:00) Set Trap 1 to -170 (캜)][]
[0 ][(07/13/11 11:48:16) PnoAcid: 20][]
[0 ][(07/13/11 11:48:22) P: AcidDrop : 1][]
[0 ][(07/13/11 11:48:36) P: AcidDrop : 2][]
[0 ][(07/13/11 11:48:50) P: AcidDrop : 3][]
[0 ][(07/13/11 11:49:00) Set Trap 1 to -170 (캜)][]
[19 ][(07/13/11 11:49:00) P: Start trapping CO2 & residual gas for 570 s][]
[0 ][(07/13/11 11:58:31) P: Gas pressure in T1 after carbonate reaction: 71][]
[19 ][(07/13/11 11:58:31) P: Waiting for HV Pump Free][]
[19 ][(07/13/11 11:58:32) P: Pumping residual gas][]
[0 ][(07/13/11 11:58:32) P: Trap 1 Temperature prior to pumping residual gas -197 캜 ][]
[0 ][(07/13/11 11:58:32) Set Trap 1 to -170 (캜)][]
[0 ][(07/13/11 11:59:02) Set Trap 1 to -90 (캜)][]
[13 ][(07/13/11 11:59:03) Turret position ( 2) Ok!][]
[6 ][(07/13/11 11:59:08) Disconnected vial at Line 1 / Position 2 ][]
[13 ][(07/13/11 11:59:26) Turret position ( 1) Ok!][]
[6 ][(07/13/11 11:59:34) Connected vial at Line 1 /Position 1 ][]
[17 ][(07/13/11 11:59:34) P: Completed Preparing Line 1 Position 2][]
[16 ][(07/13/11 11:59:36) Start PREPARATION Script 1][]
[0 ][(07/13/11 11:59:36) M: Next preparation starting...][]
[17 ][(07/13/11 11:59:36) P: Start Preparing Line 2 Position 2][]
[0 ][(07/13/11 11:59:36) P: Wait for Trap 1 free][]
[0 ][(07/13/11 11:59:36) Set Trap 1 to -90 (캜)][]
[0 ][(07/13/11 11:59:36) Set Trap 2 to 30 (캜)][]
[0 ][(07/13/11 12:02:38) M: Tot CO2 : 1038][]
[0 ][(07/13/11 12:02:38) M: Number of expansions: 0][]
[0 ][(07/13/11 12:02:38) M: CO2 after Expansion: 1038 ubar][]
[0 ][(07/13/11 12:02:38) DI: Start Reference Refill][]
[0 ][(07/13/11 12:04:25) DI: Reference Refill finished with pressure 7.9 mbar][]
[17 ][(07/13/11 12:04:30) M: Transferring CO2 to trap 2][]
[0 ][(07/13/11 12:04:30) Set Trap 2 to -30 (캜)][]
[0 ][(07/13/11 12:04:59) Set Trap 2 to -170 (캜)][]
[19 ][(07/13/11 12:05:58) M: Transfer Time][]
[0 ][(07/13/11 12:07:28) M: CO2 in T1 after transfer: 18 ubar][]
[0 ][(07/13/11 12:07:28) Set Trap 1 to 140 (캜)][]
[0 ][(07/13/11 12:07:28) Set Trap 2 to 30 (캜)][]
[18 ][(07/13/11 12:07:28) M: CO2 is transferred][]
[0 ][(07/13/11 12:07:28) Start Peak Center][]
[0 ][(07/13/11 12:07:30) Set Trap 1 to 140 (캜)][]
[8 ][(07/13/11 12:08:04) Peak Center Determination returns 62739][Forward Scan returns 62778 Reverse Scan return 62700]
[0 ][(07/13/11 12:08:04) Peak Center found at (62739)][]
[0 ][(07/13/11 12:08:21) Start Background][]
[17 ][(07/13/11 12:08:28) P: Start pumping Trap 1 for 75 s with Kiel valves 1 and 2 OFF.][]
[17 ][(07/13/11 12:09:43) P: Continue pumping Trap 1 for 75 s with Kiel valves 1 and 2 ON.][]
[0 ][(07/13/11 12:10:33) Script successfully completed][]
[0 ][(07/13/11 12:10:33) Background: 0.25 mV,0.25 mV,0.23 mV (MAT253-User)][]
[0 ][(07/13/11 12:10:33) Background finished][]
[19 ][(07/13/11 12:10:36) M: Wait for measurement temperature in T2 (30.0 C).][]
[0 ][(07/13/11 12:10:36) Set Trap 2 to 30 (캜)][]
[0 ][(07/13/11 12:10:36) M: Waiting 10 s before measuring initial signal intensity...][]
[0 ][(07/13/11 12:10:47) M: Initial signal intensity: 7681.87 mV][]
[0 ][(07/13/11 12:10:47) Start Pressure Adjustment][]
[0 ][(07/13/11 12:10:47) PressAdjust master level : PRESS_AD_CAPILLARY][]
[0 ][(07/13/11 12:10:58) Acid Temperature: 77.4 (캜)][]
[0 ][(07/13/11 12:10:58) P: Connecting sample vial (line 2, position 2)...][]
[13 ][(07/13/11 12:10:59) Turret position ( 1) Ok!][]
[0 ][(07/13/11 12:11:03) Determine decay 9.39 (mV/sec) sample intensity 7495.47 (mV)][]
[6 ][(07/13/11 12:11:04) Disconnected vial at Line 2 / Position 1 ][]
[13 ][(07/13/11 12:11:09) Turret position ( 2) Ok!][]
[0 ][(07/13/11 12:11:13) Signal up parameter 5.0000 calculated 303.4 (mV)][]
[0 ][(07/13/11 12:11:13) Calculated pressadjust level 5765.20 (mV)][]
[6 ][(07/13/11 12:11:17) Connected vial at Line 2 /Position 2 ][]
[17 ][(07/13/11 12:11:17) LT: Starting leak test.][]
[17 ][(07/13/11 12:11:17) LT: Pumpdown sample for 150 s...][]
[0 ][(07/13/11 12:12:38) Signals after pressadjust sample 6869.28 (mV) reference 5773.32 (mV)][]
[0 ][(07/13/11 12:12:38) Waiting for sample intensity reaching level][]
[1 ][(07/13/11 12:13:47) LT: Wait to reach 1000.0 (킶ar)][]
[0 ][(07/13/11 12:14:08) Pressadjust result intensity sample 6329.19 (mV) intensity reference 5773.32 (mV) intensity signal up 288.7 (mV)][]
[0 ][(07/13/11 12:14:08) Switching back to reference side][]
[0 ][(07/13/11 12:14:18) Script successfully completed][]
[0 ][(07/13/11 12:14:18) PressAdjust: L: 6329.2 R: 5773.3 ( Master Capillary )][]
[0 ][(07/13/11 12:14:18) Pressure Adjustment finished][]
[0 ][(07/13/11 12:14:18) ...Click Clack...][]
[0 ][(07/13/11 12:14:26) Start Measurement Loop][]
[0 ][(07/13/11 12:14:26) DiMeasurementLoop Cy:8 Prdl:30000 IT:8000][]
[18 ][(07/13/11 12:14:31) LT: Leak test finished. LeakRate : 576.3 킖ar/Min][]
[0 ][(07/13/11 12:14:31) Set Trap 1 to -20 (캜)][]
[0 ][(07/13/11 12:15:23) Set Trap 1 to -170 (캜)][]
[0 ][(07/13/11 12:16:52) PnoAcid: 20][]
[0 ][(07/13/11 12:16:56) P: AcidDrop : 1][]
[0 ][(07/13/11 12:17:11) P: AcidDrop : 2][]
[0 ][(07/13/11 12:17:25) P: AcidDrop : 3][]
[0 ][(07/13/11 12:17:35) Set Trap 1 to -170 (캜)][]
[19 ][(07/13/11 12:17:35) P: Start trapping CO2 & residual gas for 570 s][]
[0 ][(07/13/11 12:27:01) DI: Measurement Loop finished][]
[19 ][(07/13/11 12:27:01) M: Waiting for HV Pump Free][]
[17 ][(07/13/11 12:27:03) M: Start cleaning cycle Trap 2][]
[0 ][(07/13/11 12:27:03) Set Trap 2 to 140 (캜)][]
[0 ][(07/13/11 12:27:05) P: Gas pressure in T1 after carbonate reaction: 59][]
[19 ][(07/13/11 12:27:06) P: Waiting for HV Pump Free][]
[0 ][(07/13/11 12:29:04) M: Start pumping Trap 2][]
[18 ][(07/13/11 12:31:35) M: End of cleaning cycle Trap 2][]
[0 ][(07/13/11 12:31:35) Set Trap 2 to 30 (캜)][]
[19 ][(07/13/11 12:31:36) P: Pumping residual gas][]
[0 ][(07/13/11 12:31:36) P: Trap 1 Temperature prior to pumping residual gas -196 캜 ][]
[0 ][(07/13/11 12:31:36) Set Trap 1 to -170 (캜)][]
[17 ][(07/13/11 12:31:37) M: Finished Measuring Line 1 Sample 2][]
[1 ][(07/13/11 12:31:37) CleanUp Script terminates now][]
[37 ][(07/13/11 12:31:37) Action Thread Done>][23.876]
[16 ][(07/13/11 12:31:38) Sample ISL Script 1][]
[1 ][(07/13/11 12:31:39) CleanUp Script terminates now][]
[17 ][(07/13/11 12:31:39) Start New Carbonate Acquisition script][]
[0 ][(07/13/11 12:31:39) Set Trap 2 to 30 (캜)][]
[17 ][(07/13/11 12:31:39) M: Start Measuring Line 2 Sample 2 - Wait for Prep ready][]
[0 ][(07/13/11 12:32:06) Set Trap 1 to -90 (캜)][]
[13 ][(07/13/11 12:32:07) Turret position ( 2) Ok!][]
[6 ][(07/13/11 12:32:14) Disconnected vial at Line 2 / Position 2 ][]
[13 ][(07/13/11 12:32:32) Turret position ( 1) Ok!][]
[6 ][(07/13/11 12:32:40) Connected vial at Line 2 /Position 1 ][]
[17 ][(07/13/11 12:32:40) P: Completed Preparing Line 2 Position 2][]
[16 ][(07/13/11 12:32:42) Start PREPARATION Script 2][]
[0 ][(07/13/11 12:32:42) M: Next preparation starting...][]
[17 ][(07/13/11 12:32:42) P: Start Preparing Line 1 Position 3][]
[0 ][(07/13/11 12:32:42) P: Wait for Trap 1 free][]
[0 ][(07/13/11 12:32:42) Set Trap 1 to -90 (캜)][]
[0 ][(07/13/11 12:32:42) Set Trap 2 to 30 (캜)][]
[0 ][(07/13/11 12:35:44) M: Tot CO2 : 797][]
[0 ][(07/13/11 12:35:44) M: Number of expansions: 0][]
[0 ][(07/13/11 12:35:44) M: CO2 after Expansion: 797 ubar][]
[1 ][(07/13/11 12:35:44) DI: Reference Refill skipped][]
[17 ][(07/13/11 12:35:50) M: Transferring CO2 to trap 2][]
[0 ][(07/13/11 12:35:50) Set Trap 2 to -30 (캜)][]
[0 ][(07/13/11 12:36:30) Set Trap 2 to -170 (캜)][]
[19 ][(07/13/11 12:37:58) M: Transfer Time][]
[0 ][(07/13/11 12:39:28) M: CO2 in T1 after transfer: 18 ubar][]
[0 ][(07/13/11 12:39:28) Set Trap 1 to 140 (캜)][]
[0 ][(07/13/11 12:39:28) Set Trap 2 to 30 (캜)][]
[18 ][(07/13/11 12:39:28) M: CO2 is transferred][]
[0 ][(07/13/11 12:39:28) Start Peak Center][]
[0 ][(07/13/11 12:39:30) Set Trap 1 to 140 (캜)][]
[8 ][(07/13/11 12:40:03) Peak Center Determination returns 62739][Forward Scan returns 62778 Reverse Scan return 62700]
[0 ][(07/13/11 12:40:03) Peak Center found at (62739)][]
[0 ][(07/13/11 12:40:20) Background: BGD 2011/Jul/13 12:10 - ,0.25 mV,0.25 mV,0.23 mV (MAT253-User)][]
[19 ][(07/13/11 12:40:22) M: Wait for measurement temperature in T2 (30.0 C).][]
[0 ][(07/13/11 12:40:22) Set Trap 2 to 30 (캜)][]
[0 ][(07/13/11 12:40:22) M: Waiting 10 s before measuring initial signal intensity...][]
[17 ][(07/13/11 12:40:26) P: Start pumping Trap 1 for 75 s with Kiel valves 1 and 2 OFF.][]
[0 ][(07/13/11 12:40:33) M: Initial signal intensity: 3385.96 mV][]
[0 ][(07/13/11 12:40:33) Start Pressure Adjustment][]
[0 ][(07/13/11 12:40:33) PressAdjust master level : PRESS_AD_CAPILLARY][]
[0 ][(07/13/11 12:40:49) Determine decay 2.59 (mV/sec) sample intensity 3343.28 (mV)][]
[0 ][(07/13/11 12:40:59) Signal up parameter 5.0000 calculated 147.8 (mV)][]
[0 ][(07/13/11 12:40:59) Calculated pressadjust level 2808.24 (mV)][]
[17 ][(07/13/11 12:41:41) P: Continue pumping Trap 1 for 75 s with Kiel valves 1 and 2 ON.][]
[0 ][(07/13/11 12:41:54) Signals after pressadjust sample 3175.58 (mV) reference 2823.61 (mV)][]
[0 ][(07/13/11 12:41:54) Waiting for sample intensity reaching level][]
[0 ][(07/13/11 12:42:36) Pressadjust result intensity sample 3069.42 (mV) intensity reference 2823.61 (mV) intensity signal up 141.2 (mV)][]
[0 ][(07/13/11 12:42:36) Switching back to reference side][]
[0 ][(07/13/11 12:42:46) Script successfully completed][]
[0 ][(07/13/11 12:42:47) PressAdjust: L: 3069.4 R: 2823.6 ( Master Capillary )][]
[0 ][(07/13/11 12:42:47) Pressure Adjustment finished][]
[0 ][(07/13/11 12:42:47) ...Click Clack...][]
[0 ][(07/13/11 12:42:54) Start Measurement Loop][]
[0 ][(07/13/11 12:42:54) DiMeasurementLoop Cy:8 Prdl:30000 IT:8000][]
[0 ][(07/13/11 12:42:56) Acid Temperature: 77.4 (캜)][]
[0 ][(07/13/11 12:42:56) P: Clean acid delivery tube with 1 drop into previous vial (line 1, position 2).][]
[13 ][(07/13/11 12:42:57) Turret position ( 1) Ok!][]
[6 ][(07/13/11 12:43:02) Disconnected vial at Line 1 / Position 1 ][]
[13 ][(07/13/11 12:43:07) Turret position ( 2) Ok!][]
[6 ][(07/13/11 12:43:14) Connected vial at Line 1 /Position 2 ][]
[0 ][(07/13/11 12:43:17) P: Succesful test drop at line 1][]
[0 ][(07/13/11 12:43:17) P: Connecting sample vial (line 1, position 3)...][]
[13 ][(07/13/11 12:43:18) Turret position ( 2) Ok!][]
[6 ][(07/13/11 12:43:23) Disconnected vial at Line 1 / Position 2 ][]
[13 ][(07/13/11 12:43:28) Turret position ( 3) Ok!][]
[6 ][(07/13/11 12:43:38) Connected vial at Line 1 /Position 3 ][]
[17 ][(07/13/11 12:43:38) LT: Starting leak test.][]
[17 ][(07/13/11 12:43:38) LT: Pumpdown sample for 150 s...][]
[1 ][(07/13/11 12:46:08) LT: Wait to reach 1000.0 (킶ar)][]
[18 ][(07/13/11 12:46:52) LT: Leak test finished. LeakRate : 532.4 킖ar/Min][]
[0 ][(07/13/11 12:46:52) Set Trap 1 to -20 (캜)][]
[0 ][(07/13/11 12:47:59) Set Trap 1 to -170 (캜)][]
[0 ][(07/13/11 12:49:59) Unable reach trap temperature: -160.0 (캜) Kiel IV Carbonate/Get Trap 1 Temperature : -136.2 (캜)][]
[0 ][(07/13/11 12:49:59) Switch on 'Refill direct' to increase cooling rate][]
[0 ][(07/13/11 12:52:00) PnoAcid: 23][]
[0 ][(07/13/11 12:52:01) P: AcidDrop : 1][]
[0 ][(07/13/11 12:52:14) P: AcidDrop : 2][]
[0 ][(07/13/11 12:52:28) P: AcidDrop : 3][]
[0 ][(07/13/11 12:52:38) Set Trap 1 to -170 (캜)][]
[19 ][(07/13/11 12:52:38) P: Start trapping CO2 & residual gas for 570 s][]
[0 ][(07/13/11 12:55:29) DI: Measurement Loop finished][]
[19 ][(07/13/11 12:55:29) M: Waiting for HV Pump Free][]
[17 ][(07/13/11 12:55:31) M: Start cleaning cycle Trap 2][]
[0 ][(07/13/11 12:55:31) Set Trap 2 to 140 (캜)][]
[0 ][(07/13/11 12:57:33) M: Start pumping Trap 2][]
[18 ][(07/13/11 13:00:03) M: End of cleaning cycle Trap 2][]
[0 ][(07/13/11 13:00:03) Set Trap 2 to 30 (캜)][]
[17 ][(07/13/11 13:00:05) M: Finished Measuring Line 2 Sample 2][]
[1 ][(07/13/11 13:00:05) CleanUp Script terminates now][]
[37 ][(07/13/11 13:00:05) Action Thread Done>][38.844]
[0 ][(07/13/11 13:02:09) P: Gas pressure in T1 after carbonate reaction: 49][]
[19 ][(07/13/11 13:02:09) P: Waiting for HV Pump Free][]
[19 ][(07/13/11 13:02:10) P: Pumping residual gas][]
[0 ][(07/13/11 13:02:10) P: Trap 1 Temperature prior to pumping residual gas -197 캜 ][]
[0 ][(07/13/11 13:02:10) Set Trap 1 to -170 (캜)][]
[0 ][(07/13/11 13:02:40) Set Trap 1 to -90 (캜)][]
[13 ][(07/13/11 13:02:41) Turret position ( 3) Ok!][]
[6 ][(07/13/11 13:02:46) Disconnected vial at Line 1 / Position 3 ][]
[13 ][(07/13/11 13:03:03) Turret position ( 1) Ok!][]
[6 ][(07/13/11 13:03:11) Connected vial at Line 1 /Position 1 ][]
[17 ][(07/13/11 13:03:11) P: Completed Preparing Line 1 Position 3][]
[16 ][(07/13/11 13:03:28) Sample ISL Script 2][]
[1 ][(07/13/11 13:03:29) CleanUp Script terminates now][]
[17 ][(07/13/11 13:03:29) Start New Carbonate Acquisition script][]
[0 ][(07/13/11 13:03:29) Set Trap 2 to 30 (캜)][]
[17 ][(07/13/11 13:03:29) M: Start Measuring Line 1 Sample 3 - Wait for Prep ready][]
[16 ][(07/13/11 13:03:31) Start PREPARATION Script 3][]
[0 ][(07/13/11 13:03:31) M: Next preparation starting...][]
[17 ][(07/13/11 13:03:31) P: Start Preparing Line 2 Position 3][]
[0 ][(07/13/11 13:03:31) P: Wait for Trap 1 free][]
[0 ][(07/13/11 13:03:31) Set Trap 1 to -90 (캜)][]
[0 ][(07/13/11 13:03:35) Set Trap 2 to 30 (캜)][]
[0 ][(07/13/11 13:06:37) M: Tot CO2 : 997][]
[0 ][(07/13/11 13:06:37) M: Number of expansions: 0][]
[0 ][(07/13/11 13:06:37) M: CO2 after Expansion: 997 ubar][]
[1 ][(07/13/11 13:06:37) DI: Reference Refill skipped][]
[17 ][(07/13/11 13:06:40) M: Transferring CO2 to trap 2][]
[0 ][(07/13/11 13:06:40) Set Trap 2 to -30 (캜)][]
[0 ][(07/13/11 13:07:04) Set Trap 2 to -170 (캜)][]
[19 ][(07/13/11 13:08:01) M: Transfer Time][]
[0 ][(07/13/11 13:09:32) M: CO2 in T1 after transfer: 18 ubar][]
[0 ][(07/13/11 13:09:32) Set Trap 1 to 140 (캜)][]
[0 ][(07/13/11 13:09:32) Set Trap 2 to 30 (캜)][]
[18 ][(07/13/11 13:09:32) M: CO2 is transferred][]
[0 ][(07/13/11 13:09:32) Start Peak Center][]
[0 ][(07/13/11 13:09:33) Set Trap 1 to 140 (캜)][]
[8 ][(07/13/11 13:10:07) Peak Center Determination returns 62739][Forward Scan returns 62778 Reverse Scan return 62700]
[0 ][(07/13/11 13:10:07) Peak Center found at (62739)][]
[0 ][(07/13/11 13:10:24) Background: BGD 2011/Jul/13 12:10 - ,0.25 mV,0.25 mV,0.23 mV (MAT253-User)][]
[19 ][(07/13/11 13:10:26) M: Wait for measurement temperature in T2 (30.0 C).][]
[0 ][(07/13/11 13:10:26) Set Trap 2 to 30 (캜)][]
[0 ][(07/13/11 13:10:31) M: Waiting 10 s before measuring initial signal intensity...][]
[17 ][(07/13/11 13:10:40) P: Start pumping Trap 1 for 75 s with Kiel valves 1 and 2 OFF.][]
[0 ][(07/13/11 13:10:42) M: Initial signal intensity: 6861.54 mV][]
[0 ][(07/13/11 13:10:42) Start Pressure Adjustment][]
[0 ][(07/13/11 13:10:42) PressAdjust master level : PRESS_AD_CAPILLARY][]
[0 ][(07/13/11 13:10:58) Determine decay 6.02 (mV/sec) sample intensity 6757.09 (mV)][]
[0 ][(07/13/11 13:11:08) Signal up parameter 5.0000 calculated 292.8 (mV)][]
[0 ][(07/13/11 13:11:08) Calculated pressadjust level 5562.82 (mV)][]
[17 ][(07/13/11 13:11:55) P: Continue pumping Trap 1 for 75 s with Kiel valves 1 and 2 ON.][]
[0 ][(07/13/11 13:12:54) Signals after pressadjust sample 6092.90 (mV) reference 5547.22 (mV)][]
[0 ][(07/13/11 13:12:54) Waiting for sample intensity reaching level][]
[0 ][(07/13/11 13:13:00) Pressadjust result intensity sample 6055.86 (mV) intensity reference 5547.22 (mV) intensity signal up 277.4 (mV)][]
[0 ][(07/13/11 13:13:00) Switching back to reference side][]
[0 ][(07/13/11 13:13:10) Acid Temperature: 77.4 (캜)][]
[0 ][(07/13/11 13:13:10) P: Clean acid delivery tube with 1 drop into previous vial (line 2, position 2).][]
[13 ][(07/13/11 13:13:10) Turret position ( 1) Ok!][]
[0 ][(07/13/11 13:13:10) Script successfully completed][]
[0 ][(07/13/11 13:13:11) PressAdjust: L: 6055.9 R: 5547.2 ( Master Capillary )][]
[0 ][(07/13/11 13:13:11) Pressure Adjustment finished][]
[0 ][(07/13/11 13:13:11) ...Click Clack...][]
[6 ][(07/13/11 13:13:16) Disconnected vial at Line 2 / Position 1 ][]
[0 ][(07/13/11 13:13:18) Start Measurement Loop][]
[0 ][(07/13/11 13:13:18) DiMeasurementLoop Cy:8 Prdl:30000 IT:8000][]
[13 ][(07/13/11 13:13:21) Turret position ( 2) Ok!][]
[6 ][(07/13/11 13:13:28) Connected vial at Line 2 /Position 2 ][]
[0 ][(07/13/11 13:13:32) P: Succesful test drop at line 2][]
[0 ][(07/13/11 13:13:32) P: Connecting sample vial (line 2, position 3)...][]
[13 ][(07/13/11 13:13:33) Turret position ( 2) Ok!][]
[2 ][(07/13/11 13:13:52) Unable to release vial on Line: 2][]
[2 ][(07/13/11 13:13:52) Unable to release vial on Line: 2][]
[2 ][(07/13/11 13:13:52) Sequence termination at Sample 4][]
[0 ][(07/13/11 13:25:54) DI: Measurement Loop finished][]
[19 ][(07/13/11 13:25:54) M: Waiting for HV Pump Free][]
[17 ][(07/13/11 13:25:55) M: Start cleaning cycle Trap 2][]
[0 ][(07/13/11 13:25:55) Set Trap 2 to 140 (캜)][]
[0 ][(07/13/11 13:27:57) M: Start pumping Trap 2][]
[18 ][(07/13/11 13:30:27) M: End of cleaning cycle Trap 2][]
[0 ][(07/13/11 13:30:27) Set Trap 2 to 30 (캜)][]
[17 ][(07/13/11 13:30:29) M: Finished Measuring Line 1 Sample 3][]
[1 ][(07/13/11 13:30:29) CleanUp Script terminates now][]
[37 ][(07/13/11 13:30:29) Action Thread Done>][54.956]